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Please use this identifier to cite or link to this item: http://ntour.ntou.edu.tw:8080/ir/handle/987654321/48224

Title: Facile Synthesis of Silver Nanoparticles by Electrochemical Method in the Presence of Sodium Montmorillonite
Authors: Rong-Hsin Huang
Wen-Kai Chao
Ruei-Sung Yu
R. T. Huang
Kan-Lin Hsueh
Fuh-Sheng Shieu
Contributors: 國立臺灣海洋大學:光電與材料科技學系
Date: 2012-04
Issue Date: 2018-08-16T08:05:20Z
Publisher: Journal of Electrochemical Society
Abstract: Abstract: Silver nanoparticles (AgNPs) were successfully synthesized via a rapid and convenient electrochemical method using sodium montmorillonite (MMT), a naturally occurring mineral, as both a stabilizer and a carrier. X-ray diffraction results showed that the AgNPs had face-centered cubic crystal structure. Inductively coupled plasma-atomic emission spectral analysis indicated that the AgNP yield increased with increasing the reduction potential. UV-vis absorption curves demonstrated that the AgNPs had optical absorbance at ca. 412 nm and showed a spectral blue-shift resulting from a decrease in the particle size. Transmission electron microscopy confirmed that after a centrifugation clarification process, the AgNPs formed in the aqueous solutions at reduction potentials of 5, 10, 15, and 20 V had average sizes of 4.2, 5.6, 15.3, and 20.5 nm, respectively. In contrast, in the as-prepared AgNP/MMT aqueous solutions, the AgNPs on the MMT surface had average sizes of 5.1, 8.0, 17.0, and 25.0 nm at reduction potentials of 5, 10, 15, and 20 V, respectively. Measurement of the inhibition area of antibacterial activity demonstrated that the AgNP/MMT nanocomposites had promising antibacterial applications.
Relation: 159(6) pp.122-126
URI: http://ntour.ntou.edu.tw:8080/ir/handle/987654321/48224
Appears in Collections:[光電科學研究所] 期刊論文

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